| Experiment | |
|---|---|
Method _exptl.method | X-RAY DIFFRACTION |
Source type _diffrn_source.source | SYNCHROTRON |
Source details _diffrn_source.type | NSLS BEAMLINE X8C |
Synchrotron site _diffrn_source.pdbx_synchrotron_site | NSLS |
Beamline _diffrn_source.pdbx_synchrotron_beamline | X8C |
Temperature [K] _diffrn.ambient_temp | 108 |
Detector technology _diffrn_detector.detector | CCD |
Collection date _diffrn_detector.pdbx_collection_date | 1995-06-15 |
| Software | |
Data reduction _software.classification | MADNES |
Refinement _software.classification | X-PLOR |
| General information | |
Spacegroup name _symmetry.space_group_name_H-M | P 65 2 2 |
Unit cell parameters _cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma} | 67.2 67.2 243.7 90.0 90.0 120.0 |
Wavelength _diffrn_radiation_wavelength.wavelength | 1.00615 Å |
| Refinement | |
|---|---|
PDB entry ID _entry.id | 1CWN |
Deposition date _pdbx_database_status.recvd_initial_deposition_date | 1996-07-30 |
Resolution _refine.ls_d_res_low _refine.ls_d_res_high | 6.0 - 2.000 Å |
R _refine.ls_R_factor_obs | 0.2000 |
Rwork _refine.ls_R_factor_R_work | 0.2000 WARNING: no Rfree given? |