Data quality metrics extracted from 1cly.cif.gz by aB_cif2table1 from BUSTER (Global Phasing Ltd.). See also the PDBx/mmCIF dictionary and a MXLIMS-compatible JSON representation.

Experimental information for 1CLY at RCSB, PDBe, PDBj

Experiment
Method
_exptl.method
X-RAY DIFFRACTION
Source type
_diffrn_source.source
ROTATING ANODE
Source details
_diffrn_source.type
RIGAKU RUH2R
Temperature [K]
_diffrn.ambient_temp
295
Detector technology
_diffrn_detector.detector
IMAGE PLATE
Collection date
_diffrn_detector.pdbx_collection_date
1993-07
Detector
_diffrn_detector.type
RIGAKU RAXIS IIC
Software
Data collection
_software.classification
R-AXIS
Data reduction
_software.classification
R-AXIS
Data scaling
_software.classification
R-AXIS
Refinement
_software.classification
X-PLOR
General information
Spacegroup name
_symmetry.space_group_name_H-M
P 43 21 2
Unit cell parameters
_cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma}
81.7 81.7 166.3 90.0 90.0 90.0
Wavelength
_diffrn_radiation_wavelength.wavelength
1.54180 Å

Data quality metricsOverallOuterShell
Low resolution limit [Å] 
_reflns.d_resolution_low _reflns_shell.d_res_low
 57.800 2.750
High resolution limit [Å] 
_reflns.d_resolution_high _reflns_shell.d_res_high
 2.510 2.510
Rmerge 
_reflns.pdbx_Rmerge_I_obs _reflns_shell.Rmerge_I_obs
 0.059 0.305
  Rmeas - -
  Rpim - -
  Total number of observations - -
Total number unique 
_reflns.number_obs
 20051 -
<I/σ(I)> 
_reflns.pdbx_netI_over_sigmaI _reflns_shell.meanI_over_sigI_obs
 11.90 2.00
Completeness [%] 
_reflns.percent_possible_obs _reflns_shell.percent_possible_all
 91.7 90.8
Multiplicity 
_reflns.pdbx_redundancy
 3.0 -
  CC(1/2) - -

Refinement
PDB entry ID
_entry.id
1CLY
Deposition date
_pdbx_database_status.recvd_initial_deposition_date
1995-03-15
Resolution
_refine.ls_d_res_low _refine.ls_d_res_high
8.0 - 2.500 Å
Rwork/Rfree
_refine.ls_R_factor_R_work _refine.ls_R_factor_R_free
0.2380 / 0.2980