Experiment | |
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Method _exptl.method | X-RAY DIFFRACTION The method used in the experiment. |
Source type _diffrn_source.source | SYNCHROTRON The general class of the radiation source. |
Source details _diffrn_source.type | MPG/DESY, HAMBURG BEAMLINE BW6 The make, model or name of the source of radiation. |
Synchrotron site _diffrn_source.pdbx_synchrotron_site | MPG/DESY, HAMBURG Synchrotron site. |
Beamline _diffrn_source.pdbx_synchrotron_beamline | BW6 Synchrotron beamline. |
Temperature [K] _diffrn.ambient_temp | 277 The mean temperature in kelvins at which the intensities were |
Detector technology _diffrn_detector.detector | IMAGE PLATE The general class of the radiation detector. |
Detector _diffrn_detector.type | MARRESEARCH The make, model or name of the detector device used. |
Software | |
Data reduction _software.classification | MOSFLM The classification of the program according to its |
Data scaling #1 _software.classification | CCP4 (AGROVATA The classification of the program according to its |
Data scaling #2 _software.classification | ROTAVATA The classification of the program according to its |
Phasing _software.classification | X-PLOR (3.1) The classification of the program according to its |
Model building _software.classification | X-PLOR (3.1) The classification of the program according to its |
Refinement _software.classification | X-PLOR (3.1) The classification of the program according to its |
General information | |
Spacegroup name _symmetry.space_group_name_H-M | I 2 2 2 Hermann-Mauguin space-group symbol. Note that the |
Unit cell parameters _cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma} | 64.5 Unit-cell length a corresponding to the structure reported in 81.3 Unit-cell length b corresponding to the structure reported in 119.7 Unit-cell length c corresponding to the structure reported in 90.0 Unit-cell angle alpha of the reported structure in degrees. 90.0 Unit-cell angle beta of the reported structure in degrees. 90.0 Unit-cell angle gamma of the reported structure in degrees. |
Wavelength _diffrn_radiation_wavelength.wavelength | 0.96000 ÅThe radiation wavelength in angstroms. |
Refinement | |
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PDB entry ID _entry.id | 1CFR |
Deposition date _pdbx_database_status.recvd_initial_deposition_date | 1996-02-02 |
Resolution _refine.ls_d_res_low _refine.ls_d_res_high | 10.0 - 2.150 Å |
R _refine.ls_R_factor_obs | 0.1960 |
Rwork _refine.ls_R_factor_R_work | 0.1960 WARNING: no Rfree given? |
Structure solution method _refine.pdbx_method_to_determine_struct | MULTIPLE ISOMORPHOUS REPLACEMENT |