| Experiment | |
|---|---|
Method _exptl.method | X-RAY DIFFRACTION |
Experimental protocol _diffrn_radiation.pdbx_diffrn_protocol | SINGLE WAVELENGTH |
Source type _diffrn_source.source | SYNCHROTRON |
Source details _diffrn_source.type | CHESS BEAMLINE F1 |
Synchrotron site _diffrn_source.pdbx_synchrotron_site | CHESS |
Beamline _diffrn_source.pdbx_synchrotron_beamline | F1 |
Temperature [K] _diffrn.ambient_temp | 100 |
Detector technology _diffrn_detector.detector | CCD |
Collection date _diffrn_detector.pdbx_collection_date | 1999-01-15 |
Detector _diffrn_detector.type | PRINCETON 2K |
| Software | |
Data reduction _software.classification | DENZO |
Phasing #1 _software.classification | SnB |
Phasing #2 _software.classification | GLRF |
Phasing #3 _software.classification | TRANSF |
Phasing #4 _software.classification | ENVELOPE |
Model building #1 _software.classification | TRANSF |
Model building #2 _software.classification | ENVELOPE |
Refinement _software.classification | CNS (0.5) |
| General information | |
Spacegroup name _symmetry.space_group_name_H-M | P 1 21 1 |
Unit cell parameters _cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma} | 266.17 250.12 379.10 90.00 94.11 90.00 |
Wavelength _diffrn_radiation_wavelength.wavelength | 0.92800 Å |
| Data quality metrics | Overall | OuterShell |
|---|---|---|
Low resolution limit [Å] _reflns.d_resolution_low _reflns_shell.d_res_low | 50.000 | 3.110 |
High resolution limit [Å] _reflns.d_resolution_high _reflns_shell.d_res_high | 3.000 | 3.000 |
Rmerge _reflns.pdbx_Rmerge_I_obs _reflns_shell.Rmerge_I_obs | 0.108 | 0.150 |
| Rmeas | - | - |
| Rpim | - | - |
| Total number of observations | - | - |
Total number unique _reflns.number_obs _reflns_shell.number_unique_all | 358402 | 34921 |
| <I/σ(I)> | - | - |
Completeness [%] _reflns.percent_possible_obs _reflns_shell.percent_possible_all | 37.4 | 36.8 |
| Multiplicity | - | - |
| CC(1/2) | - | - |
| Refinement | |
|---|---|
PDB entry ID _entry.id | 1C8G |
Deposition date _pdbx_database_status.recvd_initial_deposition_date | 2000-05-05 |
Resolution _refine.ls_d_res_low _refine.ls_d_res_high | 9.0 - 3.000 Å |
R _refine.ls_R_factor_obs | 0.2450 WARNING: neither Rwork nor Rfree given |