Data quality metrics extracted from 1c8f.cif.gz by aB_cif2table1 from BUSTER (Global Phasing Ltd.). See also the PDBx/mmCIF dictionary and a MXLIMS-compatible JSON representation.

Experimental information for 1C8F at RCSB, PDBe, PDBj

Experiment
Method
_exptl.method
X-RAY DIFFRACTION
Experimental protocol
_diffrn_radiation.pdbx_diffrn_protocol
SINGLE WAVELENGTH
Source type
_diffrn_source.source
SYNCHROTRON
Source details
_diffrn_source.type
CHESS BEAMLINE F1
Synchrotron site
_diffrn_source.pdbx_synchrotron_site
CHESS
Beamline
_diffrn_source.pdbx_synchrotron_beamline
F1
Temperature [K]
_diffrn.ambient_temp
277
Detector technology
_diffrn_detector.detector
OSCILLATION CAMERA
Collection date
_diffrn_detector.pdbx_collection_date
1993-01-15
Wavelength(s) [Å]
_diffrn_source.pdbx_wavelength_list
0.9, 1.4
Software
Phasing #1
_software.classification
GLRF
Phasing #2
_software.classification
TRANSF
Phasing #3
_software.classification
ENVELOPE
Model building #1
_software.classification
TRANSF
Model building #2
_software.classification
ENVELOPE
Refinement
_software.classification
CNS (0.5)
General information
Spacegroup name
_symmetry.space_group_name_H-M
P 21 21 21
Unit cell parameters
_cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma}
380.12 379.25 350.82 90.0 90.0 90.0
Wavelength
_diffrn_radiation_wavelength.wavelength
0.900001.40000 Å

Data quality metricsOverallOuterShell
Low resolution limit [Å] 
_reflns.d_resolution_low _reflns_shell.d_res_low
 37.800 3.200
High resolution limit [Å] 
_reflns.d_resolution_high _reflns_shell.d_res_high
 2.700 3.000
Rmerge 
_reflns.pdbx_Rmerge_I_obs
 0.146 -
  Rmeas - -
  Rpim - -
  Total number of observations - -
Total number unique 
_reflns.number_obs
 547268 -
<I/σ(I)> 
_reflns.pdbx_netI_over_sigmaI
 11.20 -
Completeness [%] 
_reflns.percent_possible_obs _reflns_shell.percent_possible_all
 59.6 35.0
  Multiplicity - -
  CC(1/2) - -

Refinement
PDB entry ID
_entry.id
1C8F
Deposition date
_pdbx_database_status.recvd_initial_deposition_date
2000-05-05
Resolution
_refine.ls_d_res_low _refine.ls_d_res_high
9.0 - 3.000 Å
R
_refine.ls_R_factor_obs
0.2850
Rwork
_refine.ls_R_factor_R_work
0.2850
WARNING: no Rfree given?