| Experiment | |
|---|---|
Method _exptl.method | ELECTRON CRYSTALLOGRAPHY |
Collection date _diffrn_detector.pdbx_collection_date | 2019-06-01 |
| Software | |
Refinement _software.classification | PHENIX (1.15_3459) |
| General information | |
Spacegroup name _symmetry.space_group_name_H-M | P 1 |
Unit cell parameters _cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma} | 13.97 18.55 23.86 109.52 97.33 106.58 |
Wavelength _diffrn_radiation_wavelength.wavelength | NA |
| Data quality metrics | Overall | OuterShell |
|---|---|---|
Low resolution limit [Å] _reflns.d_resolution_low _reflns_shell.d_res_low | 7.875 | 1.100 |
High resolution limit [Å] _reflns_shell.d_res_high | - | 1.050 |
| - | - | |
Rmerge _reflns_shell.Rmerge_I_obs | - | 0.419 |
| Rmeas | - | - |
| Rpim | - | - |
| Total number of observations | - | - |
Total number unique _reflns_shell.number_unique_obs | - | 852 |
<I/σ(I)> _reflns_shell.meanI_over_sigI_obs | - | 3.04 |
Completeness [%] _reflns_shell.percent_possible_all | - | 66.9 |
Multiplicity _reflns_shell.pdbx_redundancy | - | 6.8 |
CC(1/2) _reflns_shell.pdbx_CC_half | - | 0.949 |
| Refinement | |
|---|---|
PDB entry ID _entry.id | 7C4V |
Deposition date _pdbx_database_status.recvd_initial_deposition_date | 2020-05-18 |
Resolution _refine.ls_d_res_low _refine.ls_d_res_high | 7.9 - 1.050 Å |
Rwork/Rfree _refine.ls_R_factor_R_work _refine.ls_R_factor_R_free | 0.2318 / 0.2684 |
Structure solution method _refine.pdbx_method_to_determine_struct | MOLECULAR REPLACEMENT |
Starting model (for MR) _refine.pdbx_starting_model | 1FVM |