| Experiment | |
|---|---|
Method _exptl.method | X-RAY DIFFRACTION |
Experimental protocol _diffrn_radiation.pdbx_diffrn_protocol | SINGLE WAVELENGTH |
Source type _diffrn_source.source | ROTATING ANODE |
Source details _diffrn_source.type | ELLIOTT GX-6 |
Temperature [K] _diffrn.ambient_temp | 292 |
Detector technology _diffrn_detector.detector | FILM |
Collection date _diffrn_detector.pdbx_collection_date | 1981-01-01 |
| Software | |
Data reduction _software.classification | FILME |
Data scaling _software.classification | PURDUE (DATA PROCESSING PACKAGE) |
Refinement _software.classification | FRODO |
| General information | |
Spacegroup name _symmetry.space_group_name_H-M | C 1 2 1 |
Unit cell parameters _cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma} | 317.27 304.03 184.60 90.00 94.36 90.00 |
Wavelength _diffrn_radiation_wavelength.wavelength | 1.54180 Å |
| Data quality metrics | Overall |
|---|---|
Low resolution limit [Å] _reflns.d_resolution_low | 24.730 |
High resolution limit [Å] _reflns.d_resolution_high | 2.450 |
Rmerge _reflns.pdbx_Rmerge_I_obs | 0.140 |
| Rmeas | - |
| Rpim | - |
| Total number of observations | - |
Total number unique _reflns.number_obs | 503000 |
| <I/σ(I)> | - |
Completeness [%] _reflns.percent_possible_obs | 76.0 |
Multiplicity _reflns.pdbx_redundancy | 1.6 |
| CC(1/2) | - |
| Refinement | |
|---|---|
PDB entry ID _entry.id | 2BUK |
Deposition date _pdbx_database_status.recvd_initial_deposition_date | 2005-06-14 |
Resolution _refine.ls_d_res_low _refine.ls_d_res_high | 7.5 - 2.450 Å |
Rwork _refine.ls_R_factor_R_work | 0.2730 WARNING: no Rfree given (but Rwork)!? |
Structure solution method _refine.pdbx_method_to_determine_struct | OTHER |