| Experiment | |
|---|---|
Method _exptl.method | ELECTRON CRYSTALLOGRAPHY |
Detector technology _diffrn_detector.detector | FILM |
Collection date _diffrn_detector.pdbx_collection_date | 1986-01-01 |
| Software | |
Data reduction #1 _software.classification | PICKYCOR |
Data reduction #2 _software.classification | AN (MRC ELECTRON DIFFRACTION PROGRAM) |
Refinement _software.classification | PROLSQ |
| General information | |
Spacegroup name _symmetry.space_group_name_H-M | P 3 |
Unit cell parameters _cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma} | 62.45 62.45 100.90 90.0 90.0 120.0 |
Wavelength _diffrn_radiation_wavelength.wavelength | 0.03300 Å |
| Data quality metrics | Overall |
|---|---|
Low resolution limit [Å] _reflns.d_resolution_low | 54.000 |
High resolution limit [Å] _reflns.d_resolution_high | 2.800 |
Rmerge _reflns.pdbx_Rmerge_I_obs | 0.150 |
| Rmeas | - |
| Rpim | - |
| Total number of observations | - |
Total number unique _reflns.number_obs | 6750 |
| <I/σ(I)> | - |
Completeness [%] _reflns.percent_possible_obs | 62.3 |
Multiplicity _reflns.pdbx_redundancy | 18.0 |
| CC(1/2) | - |
| Refinement | |
|---|---|
PDB entry ID _entry.id | 2BRD |
Deposition date _pdbx_database_status.recvd_initial_deposition_date | 1995-12-27 |
Resolution _refine.ls_d_res_low _refine.ls_d_res_high | 30.0 - 3.500 Å |
Rwork _refine.ls_R_factor_R_work | 0.2800 WARNING: no Rfree given (but Rwork)!? |