| Experiment | |
|---|---|
Method _exptl.method | X-RAY DIFFRACTION |
Source details _diffrn_source.type | ENRAF-NONIUS |
Temperature [K] _diffrn.ambient_temp | 287 |
Detector technology _diffrn_detector.detector | DIFFRACTOMETER |
Collection date _diffrn_detector.pdbx_collection_date | 1985-06 |
Detector _diffrn_detector.type | ENRAF-NONIUS FAST |
| Software | |
Phasing _software.classification | X-PLOR (3.1) |
Model building _software.classification | X-PLOR (3.1) |
Refinement _software.classification | X-PLOR (3.1) |
| General information | |
Spacegroup name _symmetry.space_group_name_H-M | P 21 3 |
Unit cell parameters _cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma} | 47.9 47.9 47.9 90.0 90.0 90.0 |
Wavelength _diffrn_radiation_wavelength.wavelength | 1.54180 Å |
| Data quality metrics | Overall |
|---|---|
Low resolution limit [Å] _reflns.d_resolution_low | 6.000 |
High resolution limit [Å] _reflns.d_resolution_high | 3.000 |
| Rmerge | - |
| Rmeas | - |
| Rpim | - |
| Total number of observations | - |
| Total number unique | - |
| <I/σ(I)> | - |
| Completeness [%] | - |
Multiplicity _reflns.pdbx_redundancy | 1.0 |
| CC(1/2) | - |
| Refinement | |
|---|---|
PDB entry ID _entry.id | 1BH0 |
Deposition date _pdbx_database_status.recvd_initial_deposition_date | 1998-06-11 |
Resolution _refine.ls_d_res_low _refine.ls_d_res_high | 6.0 - 3.000 Å |
Structure solution method _refine.pdbx_method_to_determine_struct | ISOMORPHOUS TO EXISTING NATIVE GLUCAGON STRUCTURE |