| Experiment | |
|---|---|
Method _exptl.method | X-RAY DIFFRACTION |
Source type _diffrn_source.source | ROTATING ANODE |
Source details _diffrn_source.type | RIGAKU RUH2R |
Temperature [K] _diffrn.ambient_temp | 288 |
Detector technology _diffrn_detector.detector | AREA DETECTOR |
Collection date _diffrn_detector.pdbx_collection_date | 1992-04 |
Detector _diffrn_detector.type | SIEMENS |
| Software | |
Data reduction #1 _software.classification | XENGEN (HOWARD |
Data reduction #2 _software.classification | NIELSEN |
Data reduction #3 _software.classification | XUONG) |
Data scaling _software.classification | XENGEN |
Phasing _software.classification | X-PLOR (2.1) |
Model building _software.classification | X-PLOR (2.1) |
Refinement _software.classification | X-PLOR (2.1) |
| General information | |
Spacegroup name _symmetry.space_group_name_H-M | P 31 2 1 |
Unit cell parameters _cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma} | 135.2 135.2 79.6 90.0 90.0 120.0 |
Wavelength _diffrn_radiation_wavelength.wavelength | 1.54180 Å |
| Data quality metrics | Overall |
|---|---|
Low resolution limit [Å] _reflns.d_resolution_low | 10.000 |
High resolution limit [Å] _reflns.d_resolution_high | 2.729 |
Rmerge _reflns.pdbx_Rmerge_I_obs | 0.092 |
| Rmeas | - |
| Rpim | - |
| Total number of observations | - |
Total number unique _reflns.number_obs | 17688 |
<I/σ(I)> _reflns.pdbx_netI_over_sigmaI | 16.60 |
Completeness [%] _reflns.percent_possible_obs | 90.5 |
Multiplicity _reflns.pdbx_redundancy | 2.9 |
| CC(1/2) | - |
| Refinement | |
|---|---|
PDB entry ID _entry.id | 1BG9 |
Deposition date _pdbx_database_status.recvd_initial_deposition_date | 1998-06-05 |
Resolution _refine.ls_d_res_low _refine.ls_d_res_high | 10.0 - 2.800 Å |
Rwork/Rfree _refine.ls_R_factor_R_work _refine.ls_R_factor_R_free | 0.1510 / 0.2490 |
Structure solution method _refine.pdbx_method_to_determine_struct | REFINEMENT DIFFERENCE FOURIER |
Starting model _refine.pdbx_starting_model | 1AMY |