| Experiment | |
|---|---|
Method _exptl.method | X-RAY DIFFRACTION |
Temperature [K] _diffrn.ambient_temp | 292.0 |
Detector technology _diffrn_detector.detector | IMAGE PLATE |
Collection date _diffrn_detector.pdbx_collection_date | 1992-08-28 |
Detector _diffrn_detector.type | RIGAKU RAXIS II |
| Software | |
Data collection _software.classification | bioteX |
Data reduction _software.classification | bioteX |
Data scaling _software.classification | bioteX |
Phasing _software.classification | MERLOT |
Refinement _software.classification | TNT |
| General information | |
Spacegroup name _symmetry.space_group_name_H-M | P 21 21 21 |
Unit cell parameters _cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma} | 45.9 44.8 52.9 90.0 90.0 90.0 |
Wavelength _diffrn_radiation_wavelength.wavelength | 1.54180 Å |
| Data quality metrics | Overall | OuterShell |
|---|---|---|
Low resolution limit [Å] _reflns.d_resolution_low _reflns_shell.d_res_low | 10.000 | 1.800 |
High resolution limit [Å] _reflns.d_resolution_high _reflns_shell.d_res_high | 1.600 | 1.600 |
Rmerge _reflns.pdbx_Rmerge_I_obs | 0.083 | - |
| Rmeas | - | - |
| Rpim | - | - |
| Total number of observations | - | - |
Total number unique _reflns.number_obs | 12318 | - |
<I/σ(I)> _reflns.pdbx_netI_over_sigmaI _reflns_shell.meanI_over_sigI_obs | 6.36 | 4.22 |
Completeness [%] _reflns.percent_possible_obs _reflns_shell.percent_possible_all | 82.0 | 61.0 |
Multiplicity _reflns.pdbx_redundancy | 6.0 | - |
| CC(1/2) | - | - |
| Refinement | |
|---|---|
PDB entry ID _entry.id | 1BEL |
Deposition date _pdbx_database_status.recvd_initial_deposition_date | 1995-12-21 |
Resolution _refine.ls_d_res_low _refine.ls_d_res_high | 10.0 - 1.600 Å |
R _refine.ls_R_factor_obs | 0.1500 WARNING: neither Rwork nor Rfree given |
Structure solution method _refine.pdbx_method_to_determine_struct | MOLECULAR REPLACEMENT |
Starting model (for MR) _refine.pdbx_starting_model | PDB ENTRY 3RN3 |