| Experiment | |
|---|---|
Method _exptl.method | X-RAY DIFFRACTION |
Experimental protocol _diffrn_radiation.pdbx_diffrn_protocol | SINGLE WAVELENGTH |
Source type _diffrn_source.source | SYNCHROTRON |
Source details _diffrn_source.type | SRS BEAMLINE PX9.6 |
Synchrotron site _diffrn_source.pdbx_synchrotron_site | SRS |
Beamline _diffrn_source.pdbx_synchrotron_beamline | PX9.6 |
Temperature [K] _diffrn.ambient_temp | 100 |
Detector technology _diffrn_detector.detector | IMAGE PLATE |
Collection date _diffrn_detector.pdbx_collection_date | 1997-12-15 |
Detector _diffrn_detector.type | MARRESEARCH |
| Software | |
Data reduction _software.classification | DENZO |
Data scaling #1 _software.classification | CCP4 (AGROVATA |
Data scaling #2 _software.classification | ROTAVATA |
Phasing #1 _software.classification | MLPHARE |
Phasing #2 _software.classification | CCP4 |
Phasing #3 _software.classification | TFFC |
Model building #1 _software.classification | CCP4 |
Model building #2 _software.classification | O |
| General information | |
Spacegroup name _symmetry.space_group_name_H-M | C 1 2 1 |
Unit cell parameters _cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma} | 148.0 148.0 105.6 90.0 123.0 90.0 |
Wavelength _diffrn_radiation_wavelength.wavelength | 0.87000 Å |
| Data quality metrics | Overall |
|---|---|
Low resolution limit [Å] _reflns.d_resolution_low | 17.600 |
High resolution limit [Å] _reflns.d_resolution_high | 5.700 |
Rmerge _reflns.pdbx_Rmerge_I_obs | 0.043 |
| Rmeas | - |
| Rpim | - |
| Total number of observations | - |
Total number unique _reflns.number_obs | 5263 |
<I/σ(I)> _reflns.pdbx_netI_over_sigmaI | 6.80 |
Completeness [%] _reflns.percent_possible_obs | 94.0 |
Multiplicity _reflns.pdbx_redundancy | 2.1 |
| CC(1/2) | - |
| Refinement | |
|---|---|
PDB entry ID _entry.id | 1BDX |
Deposition date _pdbx_database_status.recvd_initial_deposition_date | 1998-05-11 |
Structure solution method _refine.pdbx_method_to_determine_struct | MOLECULAR REPLACEMENT, MIR |
Starting model (for MR) _refine.pdbx_starting_model | 1CUK |