| Experiment | |
|---|---|
Method _exptl.method | X-RAY DIFFRACTION |
Source type _diffrn_source.source | SYNCHROTRON |
Source details _diffrn_source.type | NSLS BEAMLINE X4A |
Synchrotron site _diffrn_source.pdbx_synchrotron_site | NSLS |
Beamline _diffrn_source.pdbx_synchrotron_beamline | X4A |
Detector technology _diffrn_detector.detector | IMAGE PLATE |
Collection date _diffrn_detector.pdbx_collection_date | 1993-08-29 |
Detector _diffrn_detector.type | FUJI |
| Software | |
Data reduction _software.classification | DENZO |
Phasing _software.classification | X-PLOR |
Model building _software.classification | X-PLOR |
Refinement _software.classification | X-PLOR |
| General information | |
Spacegroup name _symmetry.space_group_name_H-M | P 21 21 2 |
Unit cell parameters _cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma} | 65.46 37.26 35.45 90.0 90.0 90.0 |
Wavelength _diffrn_radiation_wavelength.wavelength | 0.98030 Å |
| Refinement | |
|---|---|
PDB entry ID _entry.id | 1BDO |
Deposition date _pdbx_database_status.recvd_initial_deposition_date | 1995-11-21 |
Resolution _refine.ls_d_res_low _refine.ls_d_res_high | 10.0 - 1.800 Å |
R _refine.ls_R_factor_obs | 0.1890 |
Rwork _refine.ls_R_factor_R_work | 0.1890 WARNING: no Rfree given? |
Structure solution method _refine.pdbx_method_to_determine_struct | A MODIFIED MAD PROCEDURE. SOFTWARE USED : NULL STARTING MODEL FOR MOLECULAR REPLACEMENT: NULL |
Starting model (for MR) _refine.pdbx_starting_model | WARNING: no starting model (for MR) given |