Experiment | |
---|---|
Method _exptl.method | X-RAY DIFFRACTION The method used in the experiment. |
Temperature [K] _diffrn.ambient_temp | 100 The mean temperature in kelvins at which the intensities were |
Software | |
Refinement _software.classification | CNS The classification of the program according to its |
General information | |
Spacegroup name _symmetry.space_group_name_H-M | P 21 21 21 Hermann-Mauguin space-group symbol. Note that the |
Unit cell parameters _cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma} | 39.30 Unit-cell length a corresponding to the structure reported in 45.60 Unit-cell length b corresponding to the structure reported in 75.84 Unit-cell length c corresponding to the structure reported in 90.0 Unit-cell angle alpha of the reported structure in degrees. 90.0 Unit-cell angle beta of the reported structure in degrees. 90.0 Unit-cell angle gamma of the reported structure in degrees. |
Wavelength _diffrn_radiation_wavelength.wavelength | 1.54180 ÅThe radiation wavelength in angstroms. |
Data quality metrics | Overall |
---|---|
Low resolution limit [Å] _reflns.d_resolution_low | 15.000 The largest value in angstroms for the interplanar spacings |
High resolution limit [Å] _reflns.d_resolution_high | 2.100 The smallest value in angstroms for the interplanar spacings |
Rmerge _reflns.pdbx_Rmerge_I_obs | 0.043 The R value for merging intensities satisfying the observed |
Rmeas | - |
Rpim | - |
Total number of observations | - |
Total number unique _reflns.number_obs | 8216 The number of reflections in the REFLN list (not the DIFFRN_REFLN |
<I/σ(I)> | - |
Completeness [%] _reflns.percent_possible_obs | 97.0 The percentage of geometrically possible reflections represented |
Multiplicity _reflns.pdbx_redundancy | 10.0 Overall redundancy for this data set. |
CC(1/2) | - |
Refinement | |
---|---|
PDB entry ID _entry.id | 1B5L |
Deposition date _pdbx_database_status.recvd_initial_deposition_date | 1999-01-07 |