Experiment | |
---|---|
Method _exptl.method | X-RAY DIFFRACTION The method used in the experiment. |
Experimental protocol _diffrn_radiation.pdbx_diffrn_protocol | SINGLE WAVELENGTH SINGLE WAVELENGTH, LAUE, or MAD. |
Software | |
Refinement _software.classification | REFMAC (5.2.0005) The classification of the program according to its |
General information | |
Spacegroup name _symmetry.space_group_name_H-M | P 21 21 21 Hermann-Mauguin space-group symbol. Note that the |
Unit cell parameters _cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma} | 60.972 Unit-cell length a corresponding to the structure reported in 102.047 Unit-cell length b corresponding to the structure reported in 146.423 Unit-cell length c corresponding to the structure reported in 90.0 Unit-cell angle alpha of the reported structure in degrees. 90.0 Unit-cell angle beta of the reported structure in degrees. 90.0 Unit-cell angle gamma of the reported structure in degrees. |
Wavelength _diffrn_radiation_wavelength.wavelength | NA |
Refinement | |
---|---|
PDB entry ID _entry.id | 2B08 |
Deposition date _pdbx_database_status.recvd_initial_deposition_date | 2005-09-13 |
Resolution _refine.ls_d_res_low _refine.ls_d_res_high | 84.5 - 1.900 Å |
Rwork/Rfree _refine.ls_R_factor_R_work _refine.ls_R_factor_R_free | 0.1767 / 0.2200 |
Structure solution method _refine.pdbx_method_to_determine_struct | FOURIER SYNTHESIS |