Data quality metrics extracted from 2ao2.cif.gz by aB_cif2table1 from BUSTER (Global Phasing Ltd.). See also the PDBx/mmCIF dictionary and a MXLIMS-compatible JSON representation.

Experimental information for 2AO2 at RCSB, PDBe, PDBj

Experiment
Method
_exptl.method
X-RAY DIFFRACTION
Experimental protocol
_diffrn_radiation.pdbx_diffrn_protocol
MAD
Source type
_diffrn_source.source
SYNCHROTRON
Source details
_diffrn_source.type
SPRING-8 BEAMLINE BL41XU
Synchrotron site
_diffrn_source.pdbx_synchrotron_site
SPring-8
Beamline
_diffrn_source.pdbx_synchrotron_beamline
BL41XU
Collection date
_diffrn_detector.pdbx_collection_date
2005-03-15
Wavelength(s) [Å]
_diffrn_source.pdbx_wavelength_list
0.97955, 0.97975, 0.98090
Software
Refinement
_software.classification
REFMAC (5.2.0005; Murshudov, G.N.; ccp4@dl.ac.uk)
General information
Spacegroup name
_symmetry.space_group_name_H-M
C 1 2 1
Unit cell parameters
_cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma}
124.452 83.840 62.671 90.00 93.36 90.00
Wavelength
_diffrn_radiation_wavelength.wavelength
1.000000.979550.979750.98090 Å

Data quality metricsOverall
Low resolution limit [Å] 
_reflns.d_resolution_low
 69.500
High resolution limit [Å] 
_reflns.d_resolution_high
 2.070
  Rmerge -
  Rmeas -
  Rpim -
  Total number of observations -
Total number unique 
_reflns.number_obs
 36542
  <I/σ(I)> -
  Completeness [%] -
  Multiplicity -
  CC(1/2) -

Refinement
PDB entry ID
_entry.id
2AO2
Deposition date
_pdbx_database_status.recvd_initial_deposition_date
2005-08-12
Resolution
_refine.ls_d_res_low _refine.ls_d_res_high
47.3 - 2.070 Å
Rwork/Rfree
_refine.ls_R_factor_R_work _refine.ls_R_factor_R_free
0.1780 / 0.2240
Structure solution method
_refine.pdbx_method_to_determine_struct
MAD