Data quality metrics extracted from 2amh.cif.gz by aB_cif2table1 from BUSTER (Global Phasing Ltd.). See also the PDBx/mmCIF dictionary and a MXLIMS-compatible JSON representation.

Experimental information for 2AMH at RCSB, PDBe, PDBj

Experiment
Method
_exptl.method
X-RAY DIFFRACTION
Experimental protocol
_diffrn_radiation.pdbx_diffrn_protocol
MAD
Source type
_diffrn_source.source
SYNCHROTRON
Source details
_diffrn_source.type
SSRL BEAMLINE BL1-5
Synchrotron site
_diffrn_source.pdbx_synchrotron_site
SSRL
Beamline
_diffrn_source.pdbx_synchrotron_beamline
BL1-5
Temperature [K]
_diffrn.ambient_temp
100
Detector technology
_diffrn_detector.detector
CCD
Collection date
_diffrn_detector.pdbx_collection_date
2005-05-15
Detector
_diffrn_detector.type
ADSC QUANTUM 4
Wavelength(s) [Å]
_diffrn_source.pdbx_wavelength_list
0.9794, 0.9796, 0.9537
Software
Data collection
_software.classification
Blu-Ice
Data scaling #1
_software.classification
SCALA (Phil Evans; pre@mrc-lmb.cam.ac.uk)
Data scaling #2
_software.classification
CCP4 (SCALA)
Phasing #1
_software.classification
SOLVE (2.08; 14-Sept-2004; Tom Terwilliger; terwilliger@LANL.gov)
Phasing #2
_software.classification
RESOLVE (2.08; 14-Sept-2004; Terwilliger, T. C; terwilliger@LANL.gov)
Refinement
_software.classification
REFMAC (Murshudov, G.N.; ccp4@dl.ac.uk)
General information
Spacegroup name
_symmetry.space_group_name_H-M
I 4
Unit cell parameters
_cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma}
97.068 97.068 48.894 90.0 90.0 90.0
Wavelength
_diffrn_radiation_wavelength.wavelength
0.979100.979400.979600.95370 Å

Data quality metricsOverall
Low resolution limit [Å] 
_reflns.d_resolution_low
 18.000
High resolution limit [Å] 
_reflns.d_resolution_high
 2.000
Rmerge 
_reflns.pdbx_Rmerge_I_obs
 0.073
  Rmeas -
  Rpim -
  Total number of observations -
Total number unique 
_reflns.number_obs
 15517
<I/σ(I)> 
_reflns.pdbx_netI_over_sigmaI
 6.50
Completeness [%] 
_reflns.percent_possible_obs
 99.8
Multiplicity 
_reflns.pdbx_redundancy
 7.0
  CC(1/2) -

Refinement
PDB entry ID
_entry.id
2AMH
Deposition date
_pdbx_database_status.recvd_initial_deposition_date
2005-08-09
Resolution
_refine.ls_d_res_low _refine.ls_d_res_high
18.0 - 2.000 Å
Rwork/Rfree
_refine.ls_R_factor_R_work _refine.ls_R_factor_R_free
0.1970 / 0.2310
Structure solution method
_refine.pdbx_method_to_determine_struct
MAD