| Experiment | |
|---|---|
Method _exptl.method | X-RAY DIFFRACTION |
Source type _diffrn_source.source | ROTATING ANODE |
Source details _diffrn_source.type | RIGAKU RUH3R |
Temperature [K] _diffrn.ambient_temp | 293 |
Detector technology _diffrn_detector.detector | IMAGE PLATE |
Collection date _diffrn_detector.pdbx_collection_date | 1995-11-22 |
Detector _diffrn_detector.type | RIGAKU |
| Software | |
Data reduction _software.classification | PROCESS |
Data scaling _software.classification | PROCESS |
Phasing _software.classification | PHASES |
Refinement _software.classification | X-PLOR (3.1) |
| General information | |
Spacegroup name _symmetry.space_group_name_H-M | P 21 21 2 |
Unit cell parameters _cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma} | 55.74 122.75 75.51 90.0 90.0 90.0 |
Wavelength _diffrn_radiation_wavelength.wavelength | 1.54180 Å |
| Data quality metrics | Overall |
|---|---|
Low resolution limit [Å] _reflns.d_resolution_low | 122.500 |
High resolution limit [Å] _reflns.d_resolution_high | 2.380 |
Rmerge _reflns.pdbx_Rmerge_I_obs | 0.043 |
| Rmeas | - |
| Rpim | - |
| Total number of observations | - |
Total number unique _reflns.number_obs | 19708 |
<I/σ(I)> _reflns.pdbx_netI_over_sigmaI | 30.48 |
Completeness [%] _reflns.percent_possible_obs | 94.8 |
Multiplicity _reflns.pdbx_redundancy | 3.3 |
| CC(1/2) | - |
| Refinement | |
|---|---|
PDB entry ID _entry.id | 1AE1 |
Deposition date _pdbx_database_status.recvd_initial_deposition_date | 1997-10-23 |
Resolution _refine.ls_d_res_low _refine.ls_d_res_high | 10.0 - 2.400 Å |
Rwork/Rfree _refine.ls_R_factor_R_work _refine.ls_R_factor_R_free | 0.1550 / 0.2480 |
Structure solution method _refine.pdbx_method_to_determine_struct | SIRAS |