| Experiment | |
|---|---|
Method _exptl.method | X-RAY DIFFRACTION |
Source type _diffrn_source.source | ROTATING ANODE |
Source details _diffrn_source.type | RIGAKU RU200 |
Temperature [K] _diffrn.ambient_temp | 298.00 |
Detector technology _diffrn_detector.detector | DIFFRACTOMETER |
Collection date _diffrn_detector.pdbx_collection_date | 1995-10 |
Detector _diffrn_detector.type | RIGAKU AFC-5R |
| Software | |
Data reduction #1 _software.classification | TEXSAN |
Data reduction #2 _software.classification | TEXRAY |
Refinement _software.classification | NUCLSQ |
| General information | |
Spacegroup name _symmetry.space_group_name_H-M | P 41 21 2 |
Unit cell parameters _cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma} | 28.13 28.13 53.56 90.0 90.0 90.0 |
Wavelength _diffrn_radiation_wavelength.wavelength | NA |
| Data quality metrics | Overall |
|---|---|
Low resolution limit [Å] _reflns.d_resolution_low | 8.000 |
High resolution limit [Å] _reflns.d_resolution_high | 1.600 |
Rmerge _reflns.pdbx_Rmerge_I_obs | 0.121 |
| Rmeas | - |
| Rpim | - |
| Total number of observations | - |
Total number unique _reflns.number_obs | 3509 |
| <I/σ(I)> | - |
| Completeness [%] | - |
| Multiplicity | - |
| CC(1/2) | - |
| Refinement | |
|---|---|
PDB entry ID _entry.id | 385D |
Deposition date _pdbx_database_status.recvd_initial_deposition_date | 1998-03-05 |
Resolution _refine.ls_d_res_low _refine.ls_d_res_high | 8.0 - 1.600 Å |
R _refine.ls_R_factor_obs | 0.2070 WARNING: no Rwork given |
Rfree _refine.ls_R_factor_R_free | 0.2170 |