| Experiment | |
|---|---|
Method _exptl.method | X-RAY DIFFRACTION |
Source type _diffrn_source.source | ROTATING ANODE |
Source details _diffrn_source.type | RIGAKU RUH2R |
Detector technology _diffrn_detector.detector | FILM |
Collection date _diffrn_detector.pdbx_collection_date | 1990 |
Detector _diffrn_detector.type | FILM |
| Software | |
Data reduction _software.classification | ROSSMANN |
Data scaling #1 _software.classification | CAMBRIDGE/ODPROC |
Data scaling #2 _software.classification | CCP4 (ROTAVATA) |
Phasing _software.classification | TNT |
Refinement _software.classification | TNT |
| General information | |
Spacegroup name _symmetry.space_group_name_H-M | P 32 2 1 |
Unit cell parameters _cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma} | 61.1 61.1 97.6 90.0 90.0 120.0 |
Wavelength _diffrn_radiation_wavelength.wavelength | 1.54180 Å |
| Data quality metrics | Overall |
|---|---|
Low resolution limit [Å] _reflns.d_resolution_low | 50.000 |
High resolution limit [Å] _reflns.d_resolution_high | 1.800 |
Rmerge _reflns.pdbx_Rmerge_I_obs | 0.052 |
| Rmeas | - |
| Rpim | - |
| Total number of observations | - |
Total number unique _reflns.number_obs | 13645 |
| <I/σ(I)> | - |
Completeness [%] _reflns.percent_possible_obs | 65.0 |
| Multiplicity | - |
| CC(1/2) | - |
| Refinement | |
|---|---|
PDB entry ID _entry.id | 256L |
Deposition date _pdbx_database_status.recvd_initial_deposition_date | 1998-02-24 |
Resolution _refine.ls_d_res_low _refine.ls_d_res_high | 30.0 - 1.800 Å |
Rwork _refine.ls_R_factor_R_work | 0.1630 WARNING: no Rfree given (but Rwork)!? |
Structure solution method _refine.pdbx_method_to_determine_struct | DIFFERENCE FOURIER |
Starting model _refine.pdbx_starting_model | WT T4LYS |