| Experiment | |
|---|---|
Method _exptl.method | X-RAY DIFFRACTION |
Detector technology _diffrn_detector.detector | IMAGE PLATE |
Collection date _diffrn_detector.pdbx_collection_date | 1994-06-13 |
Detector _diffrn_detector.type | RIGAKU RAXIS II |
| Software | |
Data reduction _software.classification | R-AXIS |
Refinement _software.classification | X-PLOR |
| General information | |
Spacegroup name _symmetry.space_group_name_H-M | P 65 2 2 |
Unit cell parameters _cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma} | 27.245 27.245 177.399 90.0 90.0 120.0 |
Wavelength _diffrn_radiation_wavelength.wavelength | NA |
| Data quality metrics | Overall |
|---|---|
Low resolution limit [Å] _reflns.d_resolution_low | 23.570 |
High resolution limit [Å] _reflns.d_resolution_high | 2.800 |
Rmerge _reflns.pdbx_Rmerge_I_obs | 0.075 |
| Rmeas | - |
| Rpim | - |
| Total number of observations | - |
Total number unique _reflns.number_obs | 1035 |
| <I/σ(I)> | - |
Completeness [%] _reflns.percent_possible_obs | 82.0 |
| Multiplicity | - |
| CC(1/2) | - |
| Refinement | |
|---|---|
PDB entry ID _entry.id | 247D |
Deposition date _pdbx_database_status.recvd_initial_deposition_date | 1996-02-02 |
Resolution _refine.ls_d_res_low _refine.ls_d_res_high | 10.0 - 2.800 Å |
R _refine.ls_R_factor_obs | 0.1870 |
Rwork _refine.ls_R_factor_R_work | 0.1870 WARNING: no Rfree given? |