Experiment | |
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Method _exptl.method | X-RAY DIFFRACTION The method used in the experiment. |
Source type _diffrn_source.source | SYNCHROTRON The general class of the radiation source. |
Source details _diffrn_source.type | SRS BEAMLINE PX9.6 The make, model or name of the source of radiation. |
Synchrotron site _diffrn_source.pdbx_synchrotron_site | SRS Synchrotron site. |
Beamline _diffrn_source.pdbx_synchrotron_beamline | PX9.6 Synchrotron beamline. |
Temperature [K] _diffrn.ambient_temp | 150.00 The mean temperature in kelvins at which the intensities were |
Detector technology _diffrn_detector.detector | IMAGE PLATE The general class of the radiation detector. |
Detector _diffrn_detector.type | MARRESEARCH The make, model or name of the detector device used. |
Software | |
Data reduction #1 _software.classification | DENZO The classification of the program according to its |
Data reduction #2 _software.classification | CCP4 The classification of the program according to its |
Refinement _software.classification | SHELXL-93 The classification of the program according to its |
General information | |
Spacegroup name _symmetry.space_group_name_H-M | P 41 21 2 Hermann-Mauguin space-group symbol. Note that the |
Unit cell parameters _cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma} | 37.29 Unit-cell length a corresponding to the structure reported in 37.29 Unit-cell length b corresponding to the structure reported in 71.12 Unit-cell length c corresponding to the structure reported in 90.0 Unit-cell angle alpha of the reported structure in degrees. 90.0 Unit-cell angle beta of the reported structure in degrees. 90.0 Unit-cell angle gamma of the reported structure in degrees. |
Wavelength _diffrn_radiation_wavelength.wavelength | 0.87000 ÅThe radiation wavelength in angstroms. |
Data quality metrics | Overall |
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Low resolution limit [Å] | - |
High resolution limit [Å] _reflns.d_resolution_high | 1.400 The smallest value in angstroms for the interplanar spacings |
Rmerge _reflns.pdbx_Rmerge_I_obs | 0.036 The R value for merging intensities satisfying the observed |
Rmeas | - |
Rpim | - |
Total number of observations | - |
Total number unique _reflns.number_obs | 10306 The number of reflections in the REFLN list (not the DIFFRN_REFLN |
<I/σ(I)> | - |
Completeness [%] | - |
Multiplicity | - |
CC(1/2) | - |
Refinement | |
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PDB entry ID _entry.id | 245D |
Deposition date _pdbx_database_status.recvd_initial_deposition_date | 1996-01-12 |