| Experiment | |
|---|---|
Method _exptl.method | X-RAY DIFFRACTION |
Source type _diffrn_source.source | ROTATING ANODE |
Temperature [K] _diffrn.ambient_temp | 291.00 |
Detector technology _diffrn_detector.detector | IMAGE PLATE |
Collection date _diffrn_detector.pdbx_collection_date | 1994-05-02 |
Detector _diffrn_detector.type | MARRESEARCH |
| Software | |
Data reduction _software.classification | IPMOSFLM |
Phasing _software.classification | AMoRE |
Refinement _software.classification | X-PLOR |
| General information | |
Spacegroup name _symmetry.space_group_name_H-M | P 21 21 21 |
Unit cell parameters _cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma} | 22.238 37.010 54.100 90.0 90.0 90.0 |
Wavelength _diffrn_radiation_wavelength.wavelength | NA |
| Refinement | |
|---|---|
PDB entry ID _entry.id | 208D |
Deposition date _pdbx_database_status.recvd_initial_deposition_date | 1995-04-26 |
Resolution _refine.ls_d_res_low _refine.ls_d_res_high | 8.0 - 2.050 Å |
R _refine.ls_R_factor_obs | 0.1680 |
Rwork _refine.ls_R_factor_R_work | 0.1680 WARNING: no Rfree given? |
Structure solution method _refine.pdbx_method_to_determine_struct | MOLECULAR REPLACEMENT |
Starting model (for MR) _refine.pdbx_starting_model | BDL001 |