| Experiment | |
|---|---|
Method _exptl.method | X-RAY DIFFRACTION |
Experimental protocol _diffrn_radiation.pdbx_diffrn_protocol | SINGLE WAVELENGTH |
Source type _diffrn_source.source | ROTATING ANODE |
Temperature [K] _diffrn.ambient_temp | 298.00 |
Detector technology _diffrn_detector.detector | AREA DETECTOR |
Collection date _diffrn_detector.pdbx_collection_date | 1994-11-03 |
Detector _diffrn_detector.type | SIEMENS-NICOLET |
| Software | |
Data collection _software.classification | XENGEN (2.0) |
Data reduction _software.classification | XENGEN (2.0) |
Data scaling _software.classification | XENGEN (V. 2.0) |
Refinement _software.classification | X-PLOR |
| General information | |
Spacegroup name _symmetry.space_group_name_H-M | C 1 2 1 |
Unit cell parameters _cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma} | 33.38 25.33 28.11 90.00 120.45 90.00 |
Wavelength _diffrn_radiation_wavelength.wavelength | NA |
| Data quality metrics | Overall |
|---|---|
Low resolution limit [Å] _reflns.d_resolution_low | 999.900 |
High resolution limit [Å] _reflns.d_resolution_high | 1.600 |
Rmerge _reflns.pdbx_Rsym_value | 0.014 |
| Rmeas | - |
| Rpim | - |
| Total number of observations | - |
Total number unique _reflns.number_obs | 1291 |
| <I/σ(I)> | - |
Completeness [%] _reflns.percent_possible_obs | 73.0 |
Multiplicity _reflns.pdbx_redundancy | 1.4 |
| CC(1/2) | - |
| Refinement | |
|---|---|
PDB entry ID _entry.id | 304D |
Deposition date _pdbx_database_status.recvd_initial_deposition_date | 1997-01-03 |
R _refine.ls_R_factor_obs | 0.1840 |
Rwork _refine.ls_R_factor_R_work | 0.1840 WARNING: no Rfree given? |
Structure solution method _refine.pdbx_method_to_determine_struct | MOLECULAR REPLACEMENT |
Starting model (for MR) _refine.pdbx_starting_model | GDHB25 |